Technology Process of ethyl 2-(carboxymethyl)benzenesulphonate
There total 3 articles about ethyl 2-(carboxymethyl)benzenesulphonate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
tetrahydrofuran; hexane;
-78 deg C, 1h, then 0 deg C, 1h;
DOI:10.1039/P19900001611
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 5h, 2.) -78 deg C, 1h, then 0 deg C, 1h
2: n-BuLi / tetrahydrofuran; hexane / 1.5 h / -78 °C
3: 70 percent / tetrahydrofuran; hexane / -78 deg C, 1h, then 0 deg C, 1h
With
n-butyllithium;
In
tetrahydrofuran; hexane;
DOI:10.1039/P19900001611
- Guidance literature:
-
Multi-step reaction with 2 steps
1: n-BuLi / tetrahydrofuran; hexane / 1.5 h / -78 °C
2: 70 percent / tetrahydrofuran; hexane / -78 deg C, 1h, then 0 deg C, 1h
With
n-butyllithium;
In
tetrahydrofuran; hexane;
DOI:10.1039/P19900001611
