1H-4-oxa-1,9-diaza-phenanthren-2-one

Base Information

• Chemical Name: 1H-4-oxa-1,9-diaza-phenanthren-2-one
• CAS No.: 1198154-30-1
• Molecular Formula: C₁₁H₈N₂O₂
• Molecular Weight: 200.197
• Mol file: 1198154-30-1.mol

Synonyms:

Chemical Property of 1H-4-oxa-1,9-diaza-phenanthren-2-one

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

1H-4-Oxa-1,9-diaza-phenanthren-2-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1H-4-oxa-1,9-diaza-phenanthren-2-one

There total 1 articles about 1H-4-oxa-1,9-diaza-phenanthren-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3-amino-4-hydroxyquinoline (99512-72-8) + chloroacetyl chloride (79-04-9) → 1H-4-oxa-1,9-diaza-phenanthren-2-one (1198154-30-1)

Guidance literature:

3-amino-4-hydroxyquinoline; chloroacetyl chloride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Inert atmosphere;

With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 16h;

Reference yield: 10.6%

1H-4-oxa-1,9-diaza-phenanthren-2-one (1198154-30-1) → 2,3-dihydro-1H-4-oxa-1,9-diaza-phenanthrene (1198154-31-2)

Guidance literature:

1H-4-oxa-1,9-diaza-phenanthren-2-one; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃;

With water; sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 1h;

upstream raw materials:

3-amino-4-hydroxyquinoline

chloroacetyl chloride

Downstream raw materials:

2,3-dihydro-1H-4-oxa-1,9-diaza-phenanthrene

Refernces