phenacyl bromide-(ring-¹³C₆)

Base Information Edit

Chemical Name:phenacyl bromide-(ring-¹³C₆)
CAS No.:125770-90-3
Molecular Formula:C₈H₇BrO
Molecular Weight:204.981
Hs Code.:
Mol file:125770-90-3.mol

phenacyl bromide-(ring-<sup>13</sup>C<sub>6</sub>)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenacyl bromide-(ring-¹³C₆) Edit

Chemical Property:

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Technology Process of phenacyl bromide-(ring-¹³C₆)

There total 2 articles about phenacyl bromide-(ring-¹³C₆) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 125770-94-7
[13C₆]acetophenone

: 125770-90-3
phenacyl bromide-(ring-¹³C₆)

Guidance literature:: With aluminium trichloride; bromine; acetophenone; In diethyl ether; Yield given; Ambient temperature;
DOI:10.1002/(SICI)1099-1344(199612)38:12<1071::AID-JLCR924>3.0.CO;2-V

Reference yield:

: 32488-44-1
benzene-⁽¹³⁾C₆

: 598-21-0
2-Bromoacetyl bromide

: 125770-90-3
phenacyl bromide-(ring-¹³C₆)

Guidance literature:: With carbon disulfide; aluminum (III) chloride; at 45 ℃; for 0.5h;
DOI:10.1021/acs.analchem.6b02658

Reference yield:

: 125770-90-3
phenacyl bromide-(ring-¹³C₆)

: 186350-00-5
2-(acetylimino)-3-(phenacyl)thiazolidine (ring-¹³C₆)

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 2 h / Heating

2: 48 percent / pyridine / CHCl₃ / 1.7 h / Heating

With pyridine; In chloroform; acetonitrile;
DOI:10.1002/(SICI)1099-1344(199612)38:12<1071::AID-JLCR924>3.0.CO;2-V