Technology Process of C13H7F2NO2
There total 5 articles about C13H7F2NO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
bis(tri-t-butylphosphine)palladium(0); cesium fluoride; silver(l) oxide;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 16h;
Inert atmosphere;
DOI:10.1039/c4cc03612c
- Guidance literature:
-
Multi-step reaction with 5 steps
1: bromine; phosphorus tribromide / hexane / 2 h / 90 °C / Inert atmosphere
2: dichloromethane / 1 h / 20 °C
3: sodium tetrahydroborate / ethanol / 20 °C / Reflux
4: selenium(IV) oxide / 1,4-dioxane / 16 h / Reflux
5: cesium fluoride; silver(l) oxide; bis(tri-t-butylphosphine)palladium(0) / N,N-dimethyl-formamide / 16 h / 100 °C / Inert atmosphere
With
selenium(IV) oxide; sodium tetrahydroborate; bis(tri-t-butylphosphine)palladium(0); bromine; phosphorus tribromide; cesium fluoride; silver(l) oxide;
In
1,4-dioxane; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c4cc03612c
- Guidance literature:
-
Multi-step reaction with 2 steps
1: selenium(IV) oxide / 1,4-dioxane / 16 h / Reflux
2: cesium fluoride; silver(l) oxide; bis(tri-t-butylphosphine)palladium(0) / N,N-dimethyl-formamide / 16 h / 100 °C / Inert atmosphere
With
selenium(IV) oxide; bis(tri-t-butylphosphine)palladium(0); cesium fluoride; silver(l) oxide;
In
1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1039/c4cc03612c