C₁₀H₁₁N₃O₃

Base Information

• Chemical Name: C₁₀H₁₁N₃O₃
• CAS No.: 1224442-42-5
• Molecular Formula: C₁₀H₁₁N₃O₃
• Molecular Weight: 221.216
• Mol file: 1224442-42-5.mol

Synonyms:

Chemical Property of C₁₀H₁₁N₃O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₀H₁₁N₃O₃

There total 1 articles about C₁₀H₁₁N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-methyl-2-nitrobenzoic acid (3113-72-2) + acetamidine (143-37-3) → C10H11N3O3 (1224442-42-5)

Guidance literature:

5-methyl-2-nitrobenzoic acid; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 0 ℃; for 1h;

acetamidine; In N,N-dimethyl-formamide; at 0 - 20 ℃;

DOI:10.1016/j.tetlet.2010.02.019

Reference yield: 95.0%

C10H11N3O3 (1224442-42-5) → 3,4-dihydro-2,6-dimethyl-4-oxoquinazoline (18731-19-6)

Guidance literature:

With palladium 10% on activated carbon; ammonium formate; acetic acid; at 20 - 80 ℃; Inert atmosphere;

DOI:10.1016/j.tetlet.2010.02.019

upstream raw materials:

5-methyl-2-nitrobenzoic acid

acetamidine

Downstream raw materials:

3,4-dihydro-2,6-dimethyl-4-oxoquinazoline

Refernces