2-(β-cyanoethyl)cyclohexanone 2,4,6-trimethylanil

Base Information

• Chemical Name: 2-(β-cyanoethyl)cyclohexanone 2,4,6-trimethylanil
• CAS No.: 117781-63-2
• Molecular Formula: C₁₈H₂₄N₂
• Molecular Weight: 268.402
• Mol file: 117781-63-2.mol

Synonyms:

Chemical Property of 2-(β-cyanoethyl)cyclohexanone 2,4,6-trimethylanil

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(β-cyanoethyl)cyclohexanone 2,4,6-trimethylanil

There total 2 articles about 2-(β-cyanoethyl)cyclohexanone 2,4,6-trimethylanil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

cyclohexanone-2-propionitrile (4594-78-9) + 2,4,6-trimethylaniline (88-05-1) → 2-(β-cyanoethyl)cyclohexanone 2,4,6-trimethylanil (117781-63-2)

Guidance literature:

zinc(II) chloride; In o-xylene; for 15h; Heating; azeotropic distillation of the water;

Reference yield:

3-[2-(2,4,6-Trimethyl-phenylamino)-cyclohex-2-enyl]-propionitrile → 2-(β-cyanoethyl)cyclohexanone 2,4,6-trimethylanil (117781-63-2)

Guidance literature:

In tetrachloromethane; at 25 ℃; for 168h; Equilibrium constant; K(tautomeric);

Reference yield:

2-(β-cyanoethyl)cyclohexanone 2,4,6-trimethylanil (117781-63-2) → 3-[2-(2,4,6-Trimethyl-phenylamino)-cyclohex-2-enyl]-propionitrile

Guidance literature:

In tetrachloromethane; at 25 ℃; for 168h; Equilibrium constant; K(tautomeric);

upstream raw materials:

cyclohexanone-2-propionitrile

2,4,6-trimethylaniline

Refernces