euphene-⁽⁸⁾

Base Information

• Chemical Name: euphene-⁽⁸⁾
• CAS No.: 516-30-3
• Molecular Formula: C₃₀H₅₂
• Molecular Weight: 412.743
• Mol file: 516-30-3.mol

Synonyms:

Chemical Property of euphene-⁽⁸⁾

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of euphene-⁽⁸⁾

There total 5 articles about euphene-⁽⁸⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tirucallen-(8)-al-(21) → tirucall-8-ene (516-30-3,6593-21-1)

Guidance literature:

With hydrazine hydrate; sodium isopentoxide; at 180 ℃;

DOI:10.1002/hlca.19430260528

Reference yield:

tirucallen-(8)-oic acid-(21)-chloride → tirucall-8-ene (516-30-3,6593-21-1)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene; palladium/barium sulfate / 90 - 100 °C / Hydrogenation

2: sodium isopentylate; hydrazine hydrate / 180 °C

With Pd-BaSO₄; hydrazine hydrate; toluene; sodium isopentoxide;

DOI:10.1002/hlca.19430260528

Reference yield:

tirucalladien-(8.24)-oic acid-(21) (28368-21-0) → tirucall-8-ene (516-30-3,6593-21-1)

Guidance literature:

Multi-step reaction with 4 steps

1: acetic acid; platinum / Hydrogenation

2: hexane; thionyl chloride

3: toluene; palladium/barium sulfate / 90 - 100 °C / Hydrogenation

4: sodium isopentylate; hydrazine hydrate / 180 °C

With Pd-BaSO₄; thionyl chloride; hexane; hydrazine hydrate; acetic acid; toluene; platinum; sodium isopentoxide;

DOI:10.1002/hlca.19430260528

upstream raw materials:

pentan-1-ol

sodium pentanolate

hydrazine hydrate

tirucalladien-(8.24)-oic acid-⁽²¹⁾

Downstream raw materials:

euphene-(8)-dione-(7.11)