mesityl-(4-phenyl-[3]pyridyl)-ketone

Base Information

• Chemical Name: mesityl-(4-phenyl-[3]pyridyl)-ketone
• CAS No.: 50770-11-1
• Molecular Formula: C₂₁H₁₉NO
• Molecular Weight: 301.388
• Mol file: 50770-11-1.mol

Synonyms:

Chemical Property of mesityl-(4-phenyl-[3]pyridyl)-ketone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of mesityl-(4-phenyl-[3]pyridyl)-ketone

There total 4 articles about mesityl-(4-phenyl-[3]pyridyl)-ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-pyridinecarbonyl chloride (10400-19-8) → mesityl-(4-phenyl-[3]pyridyl)-ketone (50770-11-1)

Guidance literature:

Multi-step reaction with 2 steps

1: aluminium chloride

2: diethyl ether / Erwaermen des Reaktionsprodukts mit Tetrachlor-<1,4>benzochinon in Benzol

With aluminium trichloride; diethyl ether;

DOI:10.1021/ja01570a046

Reference yield:

1,3,5-trimethyl-benzene (108-67-8) → mesityl-(4-phenyl-[3]pyridyl)-ketone (50770-11-1)

Guidance literature:

Multi-step reaction with 2 steps

1: aluminium chloride

2: diethyl ether / Erwaermen des Reaktionsprodukts mit Tetrachlor-<1,4>benzochinon in Benzol

With aluminium trichloride; diethyl ether;

DOI:10.1021/ja01570a046

Reference yield:

mesityl-[3]pyridyl ketone (50378-87-5) + phenylmagnesium bromide → mesityl-(4-phenyl-[3]pyridyl)-ketone (50770-11-1)

Guidance literature:

With diethyl ether; Erwaermen des Reaktionsprodukts mit Tetrachlor-<1,4>benzochinon in Benzol;

DOI:10.1021/ja01570a046

upstream raw materials:

mesityl-[3]pyridyl ketone

diethyl ether

3-pyridinecarbonyl chloride

1,3,5-trimethyl-benzene

Downstream raw materials:

9H-indeno(2,1-c)pyridin-9-one