methyl 10-methylhexadecanoate

Base Information

• Chemical Name: methyl 10-methylhexadecanoate
• CAS No.: 2490-51-9
• Molecular Formula: C₁₈H₃₆O₂
• Molecular Weight: 284.483
• Mol file: 2490-51-9.mol

Synonyms:

Chemical Property of methyl 10-methylhexadecanoate

Chemical Property:

• Boiling Point: 326.5±10.0 °C(Predicted)
• Density: 0.863±0.06 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

10-methyl Palmitic Acid methyl ester ≥98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl 10-methylhexadecanoate

There total 6 articles about methyl 10-methylhexadecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(10RS)-10-methylhexadecanol (2490-45-1) → methyl 10-methylhexadecanoate (2490-51-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 3.5 mg / CrO₃ / acetic acid / 2 h / Ambient temperature

2: 3.7 mg / diethyl ether; diethyl ether

With chromium(VI) oxide; In diethyl ether; acetic acid;

DOI:10.1021/jo00053a034

Reference yield:

10-methylhexadecyl iodide (147103-06-8) → methyl 10-methylhexadecanoate (2490-51-9)

Guidance literature:

Multi-step reaction with 4 steps

1: 6.5 mg / CH₃COOAg / acetic acid / 24 h / Heating

2: 4 mg / 0.5 M NaOMe / methanol / 0.25 h / Heating

3: 3.5 mg / CrO₃ / acetic acid / 2 h / Ambient temperature

4: 3.7 mg / diethyl ether; diethyl ether

With chromium(VI) oxide; sodium methylate; silver(I) acetate; In methanol; diethyl ether; acetic acid;

DOI:10.1021/jo00053a034

Reference yield:

10-methylhexadecyl acetate (147103-07-9) → methyl 10-methylhexadecanoate (2490-51-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 4 mg / 0.5 M NaOMe / methanol / 0.25 h / Heating

2: 3.5 mg / CrO₃ / acetic acid / 2 h / Ambient temperature

3: 3.7 mg / diethyl ether; diethyl ether

With chromium(VI) oxide; sodium methylate; In methanol; diethyl ether; acetic acid;

DOI:10.1021/jo00053a034

upstream raw materials:

3-methylnonanoic acid

azelaic monomethyl ester

diazomethane

(10RS)-10-methylhexadecanoic acid

Refernces