4-mercaptomethyl-2-phenyl-[1,3]dithiolane

Base Information

• Chemical Name: 4-mercaptomethyl-2-phenyl-[1,3]dithiolane
• CAS No.: 5694-46-2
• Molecular Formula: C₁₀H₁₂S₃
• Molecular Weight: 228.403
• Mol file: 5694-46-2.mol

Synonyms:

Chemical Property of 4-mercaptomethyl-2-phenyl-[1,3]dithiolane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-mercaptomethyl-2-phenyl-[1,3]dithiolane

There total 4 articles about 4-mercaptomethyl-2-phenyl-[1,3]dithiolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-phenyl-1,3-dithiolan-4-ylmethanol (5694-48-4) → 4-mercaptomethyl-2-phenyl-[1,3]dithiolane (5694-46-2)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether; phosphorus (III)-bromide

2: thioacetic acid; ethanol / Erwaermen des Reaktionsprodukts mit Chlorwasserstoff enthaltendem Methanol

With diethyl ether; ethanol; phosphorus tribromide; tiolacetic acid;

DOI:10.1039/jr9500002938

Reference yield:

4-bromomethyl-2-phenyl-[1,3]dithiolane (35128-29-1) + potassium thioacetate (10387-40-3) → 4-mercaptomethyl-2-phenyl-[1,3]dithiolane (5694-46-2)

Guidance literature:

With ethanol; tiolacetic acid; Erwaermen des Reaktionsprodukts mit Chlorwasserstoff enthaltendem Methanol;

DOI:10.1039/jr9500002938

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + methanol (67-56-1) + 4-(acetylmercapto-methyl)-2-phenyl-[1,3]dithiolane → 4-mercaptomethyl-2-phenyl-[1,3]dithiolane (5694-46-2)

Guidance literature:

DOI:10.1039/jr9500002938

upstream raw materials:

4-bromomethyl-2-phenyl-[1,3]dithiolane

potassium thioacetate

hydrogenchloride

methanol

Refernces

• 1、 -. "Acrylic ester compound and usage thereof". . . Retrieved 2008/06/13.