Technology Process of methyl (RS)-5-benzoyloxy-6,7-dihydroxyoctanoate
There total 6 articles about methyl (RS)-5-benzoyloxy-6,7-dihydroxyoctanoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
perchloric acid;
In
1,4-dioxane; water;
for 12h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) 50percent NaH / 1.) DMSO, 15 min, 2.) 1 h
2: 60 percent / PCC / CH2Cl2
3: Et3N / 12 h / Ambient temperature
4: 80 percent / 75-80percent MCPBA / CH2Cl2 / 18 h
5: 60 percent / Py / 3 h
6: 60 percent / 75percent HClO4 / various solvent(s); H2O; dioxane / 12 h
With
pyridine; perchloric acid; sodium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate;
In
1,4-dioxane; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 60 percent / PCC / CH2Cl2
2: Et3N / 12 h / Ambient temperature
3: 80 percent / 75-80percent MCPBA / CH2Cl2 / 18 h
4: 60 percent / Py / 3 h
5: 60 percent / 75percent HClO4 / various solvent(s); H2O; dioxane / 12 h
With
pyridine; perchloric acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate;
In
1,4-dioxane; dichloromethane; water;
