Technology Process of C25H39N2O7PS
There total 8 articles about C25H39N2O7PS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
tetrachloromethane; dichloromethane;
DOI:10.1002/cmdc.201200271
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 - 0 °C
1.2: 1 h
2.1: boron trifluoride diethyl etherate / dichloromethane / 2 h / -20 °C
3.1: 1H-imidazole / dichloromethane / 0 - 20 °C
4.1: diisobutylaluminium hydride / diethyl ether; hexane / 3 h / -78 °C
4.2: 3 h / 20 °C
4.3: 20 °C / Cooling with ice
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C
6.1: sodium carbonate / water; dichloromethane / 3 h / 0 - 20 °C
7.1: Pd(OH)2/C; hydrogen / methanol / 24 h / 20 °C / 760.05 Torr
8.1: potassium carbonate / dichloromethane; tetrachloromethane
With
1H-imidazole; oxalyl dichloride; Pd(OH)2/C; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; hydrogen; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; dimethyl sulfoxide;
In
tetrahydrofuran; methanol; tetrachloromethane; diethyl ether; hexane; dichloromethane; water;
1.1: |Swern Oxidation / 8.1: |Atherton-Todd Synthesis;
DOI:10.1002/cmdc.201200271
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Pd(OH)2/C; hydrogen / methanol / 24 h / 20 °C / 760.05 Torr
2: potassium carbonate / dichloromethane; tetrachloromethane
With
Pd(OH)2/C; hydrogen; potassium carbonate;
In
methanol; tetrachloromethane; dichloromethane;
2: |Atherton-Todd Synthesis;
DOI:10.1002/cmdc.201200271
