C₂₀H₂₀N₅O₁₃P₃S^(2-)

Base Information

• Chemical Name: C₂₀H₂₀N₅O₁₃P₃S^(2-)
• CAS No.: 118275-89-1
• Molecular Formula: C₂₀H₂₀N₅O₁₃P₃S
• Molecular Weight: 663.392
• Mol file: 118275-89-1.mol

Synonyms:

Chemical Property of C₂₀H₂₀N₅O₁₃P₃S^(2-)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of C₂₀H₂₀N₅O₁₃P₃S^(2-)

There total 3 articles about C₂₀H₂₀N₅O₁₃P₃S^(2-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C20H20N5O13P3(2-) → C20H20N5O13P3S(2-) (118275-89-1)

Guidance literature:

With sulfur; In N,N-dimethyl-formamide; for 0.166667h;

DOI:10.1021/jo00264a024

Reference yield:

N6-benzoyl-3'-(methoxyacetyl)-2'-deoxyadenosine (25152-96-9) → C20H20N5O13P3S(2-) (118275-89-1)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine / dioxane / 0.17 h

2: bis(tri-n-butylammonium) pyrophosphate, tri-n-butylamine / dimethylformamide / 0.17 h

3: sulfur / dimethylformamide / 0.17 h

With pyridine; tributyl-amine; bis(tri-n-butylammonium) pyrophosphate; sulfur; In 1,4-dioxane; N,N-dimethyl-formamide;

DOI:10.1021/jo00264a024

Reference yield:

Acetic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-(4-oxo-4H-benzo[1,3,2]dioxaphosphinin-2-yloxymethyl)-tetrahydro-furan-3-yloxymethyl ester → C20H20N5O13P3S(2-) (118275-89-1)

Guidance literature:

Multi-step reaction with 2 steps

1: bis(tri-n-butylammonium) pyrophosphate, tri-n-butylamine / dimethylformamide / 0.17 h

2: sulfur / dimethylformamide / 0.17 h

With tributyl-amine; bis(tri-n-butylammonium) pyrophosphate; sulfur; In N,N-dimethyl-formamide;

DOI:10.1021/jo00264a024

upstream raw materials:

N⁶-benzoyl-3'-(methoxyacetyl)-2'-deoxyadenosine

Downstream raw materials:

C₁₀H₁₂N₅O₁₁P₃S^(4-)

C₁₀H₁₂N₅O₁₁P₃S^(4-)

Refernces