1-(1,2-Diphenyl-ethyl)-1H-[1,2,4]triazole; compound with naphthalene-1,5-disulfonic acid

Base Information

• Chemical Name: 1-(1,2-Diphenyl-ethyl)-1H-[1,2,4]triazole; compound with naphthalene-1,5-disulfonic acid
• CAS No.: 99369-40-1
• Molecular Formula: C₁₀H₈O₆S₂*2C₁₆H₁₅N₃
• Molecular Weight: 786.932
• Mol file: 99369-40-1.mol

Synonyms:

Chemical Property of 1-(1,2-Diphenyl-ethyl)-1H-[1,2,4]triazole; compound with naphthalene-1,5-disulfonic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(1,2-Diphenyl-ethyl)-1H-[1,2,4]triazole; compound with naphthalene-1,5-disulfonic acid

There total 3 articles about 1-(1,2-Diphenyl-ethyl)-1H-[1,2,4]triazole; compound with naphthalene-1,5-disulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-benzyl-1,2,4-triazole (6085-94-5) → 1-(1,2-Diphenyl-ethyl)-1H-[1,2,4]triazole; compound with naphthalene-1,5-disulfonic acid (99369-40-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) n-C₄H₉Li / 1.) hexane, DME, -60 deg C, 10 min., 2.) -60 deg C, 1 h; room temp., 15 h

2: aq. ethanol

With n-butyllithium; In ethanol;

DOI:10.1055/s-1985-31187

Reference yield:

benzyl chloride (100-44-7) → 1-(1,2-Diphenyl-ethyl)-1H-[1,2,4]triazole; compound with naphthalene-1,5-disulfonic acid (99369-40-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) n-C₄H₉Li / 1.) hexane, DME, -60 deg C, 10 min., 2.) -60 deg C, 1 h; room temp., 15 h

2: aq. ethanol

With n-butyllithium; In ethanol;

DOI:10.1055/s-1985-31187

Reference yield:

1-(1,2-Diphenyl-ethyl)-1H-[1,2,4]triazole (99369-39-8) + naphthalene-1,5-disulfonate (81-04-9) → 1-(1,2-Diphenyl-ethyl)-1H-[1,2,4]triazole; compound with naphthalene-1,5-disulfonic acid (99369-40-1)

Guidance literature:

In ethanol;

DOI:10.1055/s-1985-31187

upstream raw materials:

1-(1,2-Diphenyl-ethyl)-1H-[1,2,4]triazole

naphthalene-1,5-disulfonate

1-benzyl-1,2,4-triazole

benzyl chloride

Refernces