N-methylcyclododecanamine

Base Information

• Chemical Name: N-methylcyclododecanamine
• CAS No.: 40221-53-2
• Molecular Formula: C₁₃H₂₇N
• Molecular Weight: 197.364
• Hs Code.: 2921300090
• European Community (EC) Number: 654-830-9
• NSC Number: 81255
• DSSTox Substance ID: DTXSID50960640
• Nikkaji Number: J308.213J
• Wikidata: Q82941872
• Mol file: 40221-53-2.mol

Synonyms:N-methylcyclododecanamine;40221-53-2;N-METHYLCYCLODODECYLAMINE;Cyclododecylamine, N-methyl-,;NSC81255;N-methyl cyclododecylamine;SCHEMBL8921740;DTXSID50960640;NSC-81255;AKOS002435286;FT-0694920;1H-Tetrazol-1-amine, 5-methyl-N-(phenylmethylene)-

Chemical Property of N-methylcyclododecanamine

Chemical Property:

• Vapor Pressure: 0.00638mmHg at 25°C
• Boiling Point: 271.6°Cat760mmHg
• Flash Point: 113.8°C
• PSA: 12.03000
• Density: 0.84g/cm³
• LogP: 4.27000
• XLogP3: 4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 197.214349865
• Heavy Atom Count: 14
• Complexity: 110

Purity/Quality:

99% ^*data from raw suppliers

N-METHYLCYCLODODECYLAMINE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CNC1CCCCCCCCCCC1

Technology Process of N-methylcyclododecanamine

There total 1 articles about N-methylcyclododecanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclododecanone (830-13-7) + methylamine (74-89-5) → N-methylcyclododecanamine (40221-53-2)

Guidance literature:

With methanol; nickel; at 120 ℃; under 88260.9 Torr; Hydrogenation;

DOI:10.1002/hlca.19550380715

Reference yield:

N-methylcyclododecanamine (40221-53-2) → 1-(2-(cyclododecyl(methyl)amino)-2-oxoethoxy)-1-methylpiperidin-1-ium iodide

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine / benzene / 3 h / 0 - 78 °C

2: 48 h / 100 °C / Sealed tube

3: methanol / 65 °C / Sealed tube

With pyridine; In methanol; benzene;

DOI:10.1007/s00044-020-02537-0

upstream raw materials:

cyclododecanone

methylamine

Refernces