6-methyldecanoic acid

Base Information

• Chemical Name: 6-methyldecanoic acid
• CAS No.: 53696-14-3
• Molecular Formula: C₁₁H₂₂O₂
• Molecular Weight: 186.294
• Hs Code.: 2915900090
• Mol file: 53696-14-3.mol

Synonyms:Capricacid, e-methyl- (4CI); 6-Methyldecanoicacid

Chemical Property of 6-methyldecanoic acid

Chemical Property:

• Vapor Pressure: 0.000557mmHg at 25°C
• Refractive Index: 1.4221 (estimate)
• Boiling Point: 289.3°Cat760mmHg
• Flash Point: 154.2°C
• PSA: 37.30000
• Density: 0.908g/cm³
• LogP: 3.45770

Purity/Quality:

99% ^*data from raw suppliers

6-METHYLDECANOIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-methyldecanoic acid

There total 17 articles about 6-methyldecanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4-methyl-octyl)-malonic acid diethyl ester → 6-methyldecanoic acid (53696-14-3)

Guidance literature:

Verseifen und Decarboxylieren;

Reference yield:

2-methylhexan-1-ol (624-22-6) → 6-methyldecanoic acid (53696-14-3)

Guidance literature:

Multi-step reaction with 9 steps

1.1: 11.2 g / red phosphorus; bromine / 0 - 20 °C

2.1: NaOEt / ethanol / 0.12 h / Heating

2.2: ethanol / 1 h / Heating

3.1: KOH / ethanol / 4 h / Heating

4.1: 3 h / 190 °C

5.1: 2.00 g / LiAlH₄ / diethyl ether / 20 °C

6.1: red phosphorus; bromine / 0 - 20 °C

7.1: NaOEt / ethanol / 0.12 h / Heating

7.2: ethanol / 1 h / Heating

8.1: KOH / ethanol / 4 h / Heating

9.1: 1.1 g / 3 h / 190 °C

With phosphorus; potassium hydroxide; lithium aluminium tetrahydride; bromine; sodium ethanolate; In diethyl ether; ethanol;

DOI:10.1016/S0957-4166(02)00172-6

Reference yield:

4-methyloctan-1-ol (38514-03-3) → 6-methyldecanoic acid (53696-14-3)

Guidance literature:

Multi-step reaction with 4 steps

1.1: red phosphorus; bromine / 0 - 20 °C

2.1: NaOEt / ethanol / 0.12 h / Heating

2.2: ethanol / 1 h / Heating

3.1: KOH / ethanol / 4 h / Heating

4.1: 1.1 g / 3 h / 190 °C

With phosphorus; potassium hydroxide; bromine; sodium ethanolate; In ethanol;

DOI:10.1016/S0957-4166(02)00172-6

upstream raw materials:

3-methylheptanoic acid

Pentanedioic acid, monomethyl ester

methyl hydrogen succinate

rac-4-methyloctanoic acid

Refernces