(2RS,3RS,4SR)-4-benzylamino-2-methyl-6-oxotetrahydropyran-3-carboxylic-acid hydrochloride

Base Information Edit

Chemical Name:(2RS,3RS,4SR)-4-benzylamino-2-methyl-6-oxotetrahydropyran-3-carboxylic-acid hydrochloride
CAS No.:77120-93-5
Molecular Formula:C₁₄H₁₇NO₄*ClH
Molecular Weight:299.754
Hs Code.:
Mol file:77120-93-5.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2RS,3RS,4SR)-4-benzylamino-2-methyl-6-oxotetrahydropyran-3-carboxylic-acid hydrochloride Edit

Chemical Property:

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Technology Process of (2RS,3RS,4SR)-4-benzylamino-2-methyl-6-oxotetrahydropyran-3-carboxylic-acid hydrochloride

There total 7 articles about (2RS,3RS,4SR)-4-benzylamino-2-methyl-6-oxotetrahydropyran-3-carboxylic-acid hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 90210-81-4,90244-05-6
1-benzyl-4-cyanomethyl-3-(1'-hydroxyethyl)azetidin-2-one

: 77120-93-5,79814-45-2,93712-44-8,102419-19-2
(2RS,3RS,4SR)-4-benzylamino-2-methyl-6-oxotetrahydropyran-3-carboxylic-acid hydrochloride

Guidance literature:: With hydrogenchloride; for 3h; Heating;

Reference yield:

: 77120-90-2
3-Benzylamino-2-pentenedioic acid diethyl ester

: 77120-93-5,79814-45-2,93712-44-8,102419-19-2
(2R,3R,4S)-4-Benzylamino-2-methyl-6-oxo-tetrahydro-pyran-3-carboxylic acid; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: toluene

2: NaBH₃CN / acetic acid

3: cc. HCl / Heating

With hydrogenchloride; sodium cyanoborohydride; In acetic acid; toluene;
DOI:10.1016/S0040-4039(00)78606-0

Reference yield:

: 77120-91-3
(E)-2-Acetyl-3-benzylamino-pent-2-enedioic acid diethyl ester

: 77120-93-5,79814-45-2,93712-44-8,102419-19-2
(2R,3R,4S)-4-Benzylamino-2-methyl-6-oxo-tetrahydro-pyran-3-carboxylic acid; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₃CN / acetic acid

2: cc. HCl / Heating

With hydrogenchloride; sodium cyanoborohydride; In acetic acid;
DOI:10.1016/S0040-4039(00)78606-0