diethanolamine [(1R)-1-acetamido-2-phenylethyl]boronate

Base Information

• Chemical Name: diethanolamine [(1R)-1-acetamido-2-phenylethyl]boronate
• CAS No.: 173937-87-6
• Molecular Formula: C₁₄H₂₁BN₂O₃
• Molecular Weight: 276.143
• Mol file: 173937-87-6.mol

Synonyms:

Chemical Property of diethanolamine [(1R)-1-acetamido-2-phenylethyl]boronate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of diethanolamine [(1R)-1-acetamido-2-phenylethyl]boronate

There total 1 articles about diethanolamine [(1R)-1-acetamido-2-phenylethyl]boronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

2,2'-iminobis[ethanol] (111-42-2) + (R)-1-acetamido-2-phenylethane-1-boronic acid (78902-01-9) → diethanolamine [(1R)-1-acetamido-2-phenylethyl]boronate (173937-87-6)

Guidance literature:

In isopropyl alcohol; (N2); stirring (20°C, 1h), rot. evapn., MgSO4 and charcoal addn.,stirring (10 h); filtn., vac. concn., pptn. (CH2Cl2, Et2O); HRMS;

DOI:10.1021/ja952816j

upstream raw materials:

2,2'-iminobis[ethanol]

(R)-1-acetamido-2-phenylethane-1-boronic acid

Refernces