4-n-butylbenzoic acid 2,2-dichloroethyl ester

Base Information

• Chemical Name: 4-n-butylbenzoic acid 2,2-dichloroethyl ester
• CAS No.: 1613638-95-1
• Molecular Formula: C₁₃H₁₆Cl₂O₂
• Molecular Weight: 275.175
• Mol file: 1613638-95-1.mol

Synonyms:

Chemical Property of 4-n-butylbenzoic acid 2,2-dichloroethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 4-n-butylbenzoic acid 2,2-dichloroethyl ester

There total 1 articles about 4-n-butylbenzoic acid 2,2-dichloroethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-butyl benzoic acid (20651-71-2) → 4-n-butylbenzoic acid 2,2-dichloroethyl ester (1613638-95-1)

Guidance literature:

Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 21 h / 0 - 20 °C

2: 10% Pt/activated carbon; hydrogen; tri-n-butyl-tin hydride / N,N-dimethyl acetamide / 2 h / 25 °C / 760.05 Torr

With dmap; 10% Pt/activated carbon; hydrogen; tri-n-butyl-tin hydride; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl acetamide;

DOI:10.1016/j.tet.2014.04.098

upstream raw materials:

4-butyl benzoic acid

Refernces