C₂₇H₃₅NO

Base Information

• Chemical Name: C₂₇H₃₅NO
• CAS No.: 63796-47-4
• Molecular Formula: C₂₇H₃₅NO
• Molecular Weight: 389.581
• Mol file: 63796-47-4.mol

Synonyms:

Chemical Property of C₂₇H₃₅NO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₃₅NO

There total 5 articles about C₂₇H₃₅NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dehydroabietic acid chloride (22478-66-6) + o-toluidine (95-53-4) → C27H35NO (63796-47-4)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 12.5h;

DOI:10.1021/acs.jafc.0c00562

Reference yield:

dehydroabietic acid (1740-19-8) → C27H35NO (63796-47-4)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride / dichloromethane / Reflux

2: triethylamine / dichloromethane / 12.5 h / 20 °C

With thionyl chloride; triethylamine; In dichloromethane;

DOI:10.1021/acs.jafc.0c00562

Reference yield:

abietic acid (514-10-3) → C27H35NO (63796-47-4)

Guidance literature:

Multi-step reaction with 3 steps

1: platinum on activated charcoal / 280 °C / Inert atmosphere

2: thionyl chloride / dichloromethane / Reflux

3: triethylamine / dichloromethane / 12.5 h / 20 °C

With thionyl chloride; platinum on activated charcoal; triethylamine; In dichloromethane;

DOI:10.1021/acs.jafc.0c00562

upstream raw materials:

dehydroabietic acid

dehydroabietic acid chloride

o-toluidine

abietic acid

Refernces