Technology Process of Nonanamide,
2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluoro-N-(phenylmethyl)-N-[4
-(1H-tetrazol-5-ylmethyl)phenyl]-
There total 5 articles about Nonanamide,
2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluoro-N-(phenylmethyl)-N-[4
-(1H-tetrazol-5-ylmethyl)phenyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
-
-
138901-05-0
2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluoro-N-(phenylmethyl)-N-<4-(1H-tetrazol-5-ylmethyl)phenyl>nonanamide
- Guidance literature:
-
With
sodium azide; ammonium chloride;
In
N,N-dimethyl-formamide;
at 135 ℃;
for 7h;
DOI:10.1021/jm00083a021
-
-
138901-05-0
2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluoro-N-(phenylmethyl)-N-<4-(1H-tetrazol-5-ylmethyl)phenyl>nonanamide
- Guidance literature:
-
Multi-step reaction with 4 steps
1: ethyl acetate / 15 h / 85 °C
2: ethyl acetate / 24 h / Ambient temperature
3: 3 g / K2CO3 / acetone / 42 h / Heating
4: sodium azide, ammonium chloride / dimethylformamide / 7 h / 135 °C
With
sodium azide; ammonium chloride; potassium carbonate;
In
ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm00083a021
-
-
138901-05-0
2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluoro-N-(phenylmethyl)-N-<4-(1H-tetrazol-5-ylmethyl)phenyl>nonanamide
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 3 g / K2CO3 / acetone / 42 h / Heating
2: sodium azide, ammonium chloride / dimethylformamide / 7 h / 135 °C
With
sodium azide; ammonium chloride; potassium carbonate;
In
N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm00083a021