3-mer-HCA

Base Information

• Chemical Name: 3-mer-HCA
• CAS No.: 1382735-24-1
• Molecular Formula: C₂₂H₁₈O₆
• Molecular Weight: 378.381
• Mol file: 1382735-24-1.mol

Synonyms:

Chemical Property of 3-mer-HCA

Chemical Property:

Purity/Quality:

98.5% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-mer-HCA

There total 15 articles about 3-mer-HCA which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C24H22O6 → 3-mer-HCA (1382735-24-1)

Guidance literature:

With water; lithium hydroxide; In tetrahydrofuran; at 40 ℃; for 40h;

DOI:10.1002/anie.201906606

Reference yield: 65.0%

C26H26O6 → 3-mer-HCA (1382735-24-1)

Guidance literature:

C₂₆H₂₆O₆; With boron tribromide; In dichloromethane;

With sodium hydroxide; In tetrahydrofuran; water; at 50 ℃; for 24h;

With hydrogenchloride; In water; pH=<2;

DOI:10.1021/jacs.7b04872

Reference yield:

C38H34O6 (1382734-78-2) → 3-mer-HCA (1382735-24-1)

Guidance literature:

C₃₈H₃₄O₆; With palladium on activated charcoal; hydrogen; In tetrahydrofuran; N,N-dimethyl-formamide;

With sodium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide;

upstream raw materials:

methyl 4-iodosalicylate

methyl 2-(benzyloxy)-4-iodobenzoate

methyl 2-(benzyloxy)-4-(pinacolboronic ester) benzoate

C₃₈H₃₄O₆

Refernces

• 1、 Feng, Liang,Wang, Kun-Yu,Yan, Tian-Hao,Zhou, Hong-Cai. "Porous Crystalline Spherulite Superstructures". supporting information. p. 460 - 471. Retrieved 2020/02/18.
• 2、 Zheng, Jian,Vemuri, Rama S.,Estevez, Luis,Koech, Phillip K.,Varga, Tamas,Camaioni, Donald M.,Blake, Thomas A.,McGrail, B. Peter,Motkuri, Radha Kishan. "Pore-Engineered Metal-Organic Frameworks with Excellent Adsorption of Water and Fluorocarbon Refrigerant for Cooling Applications". supporting information. p. 10601 - 10604. Retrieved 2017/08/15.