Sodium perfluorooctanoxyacetate

Base Information

• Chemical Name: Sodium perfluorooctanoxyacetate
• CAS No.: 134948-34-8
• Molecular Formula: C₁₀H₂F₁₇O₃*Na
• Molecular Weight: 516.087
• Mol file: 134948-34-8.mol

Synonyms:

Chemical Property of Sodium perfluorooctanoxyacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Sodium perfluorooctanoxyacetate

There total 3 articles about Sodium perfluorooctanoxyacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

Ethyl perfluorooctanoxyacetate (134918-65-3) → Sodium perfluorooctanoxyacetate (134948-34-8)

Guidance literature:

With sodium hydroxide; In ethanol; for 2h; Heating;

DOI:10.1016/S0022-1139(00)80195-5

Reference yield:

perfluorooctanoyl fluoride (335-66-0) → Sodium perfluorooctanoxyacetate (134948-34-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) tris(dimethylamino)sulfonium difluorotrimethylsilicate / 1.) acetonitrile, r.t., 2.) r.t., overnight

2: 73 percent / 1.137 N aq. sodium hydroxide / ethanol / 2 h / Heating

With sodium hydroxide; tris(dimethylamino)sulfonium trimethylsilyldifluoride; In ethanol;

DOI:10.1016/S0022-1139(00)80195-5

Reference yield:

sodium perfluorooctanoate (335-95-5) → Sodium perfluorooctanoxyacetate (134948-34-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 55 percent / sulfur tetrafluoride / bis-(2-methoxy-ethyl) ether / 1 h / Heating

2: 1.) tris(dimethylamino)sulfonium difluorotrimethylsilicate / 1.) acetonitrile, r.t., 2.) r.t., overnight

3: 73 percent / 1.137 N aq. sodium hydroxide / ethanol / 2 h / Heating

With sodium hydroxide; sulfur tetrafluoride; tris(dimethylamino)sulfonium trimethylsilyldifluoride; In ethanol; diethylene glycol dimethyl ether;

DOI:10.1016/S0022-1139(00)80195-5

upstream raw materials:

Ethyl perfluorooctanoxyacetate

perfluorooctanoyl fluoride

sodium perfluorooctanoate

Refernces