bibenzyl-4,4'-diyldi-acetic acid

Base Information

• Chemical Name: bibenzyl-4,4'-diyldi-acetic acid
• CAS No.: 93878-05-8
• Molecular Formula: C₁₈H₁₈O₄
• Molecular Weight: 298.339
• Mol file: 93878-05-8.mol

Synonyms:

Chemical Property of bibenzyl-4,4'-diyldi-acetic acid

Chemical Property:

Purity/Quality:

98%,99%, ^*data from raw suppliers

4,4'-DIMETHYLENEBIS(PHENYLACETIC ACID) AldrichCPR ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bibenzyl-4,4'-diyldi-acetic acid

There total 4 articles about bibenzyl-4,4'-diyldi-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4'-bis-(2-morpholino-2-thioxo-ethyl)-bibenzyl → bibenzyl-4,4'-diyldi-acetic acid (93878-05-8)

Guidance literature:

With sodium hydroxide;

DOI:10.1021/ja01156a059 DOI:10.1021/ja01127a001

Reference yield:

1,1'-(1,2-ethanediyl)bisbenzene (103-29-7) → bibenzyl-4,4'-diyldi-acetic acid (93878-05-8)

Guidance literature:

Multi-step reaction with 3 steps

1: ZnCl₂; HCl / <50

2: ethanolic solution

3: aqueous sulfuric acid / Erwaermen des Reaktionsprodukts mit wss. Kalilauge

With hydrogenchloride; sulfuric acid; zinc(II) chloride;

DOI:10.1002/hlca.193301601170

Reference yield:

bibenzyl-4,4'-diyldi-acetonitrile (409111-26-8) → bibenzyl-4,4'-diyldi-acetic acid (93878-05-8)

Guidance literature:

With sulfuric acid; Erwaermen des Reaktionsprodukts mit wss. Kalilauge;

DOI:10.1002/hlca.193301601170

upstream raw materials:

bibenzyl-4,4'-diyldi-acetonitrile

1,2-bis<4-(chloromethyl)phenyl>ethane

1,1'-(1,2-ethanediyl)bisbenzene

Downstream raw materials:

bibenzyl-4,4'-diyl-di-acetic acid dimethyl ester

bibenzyl-4,4'-diyl-di-acetic acid diethyl ester