4(1H)-Pyridinone, 1-hydroxy-3,5-dinitro-, compd. with pyridine (2:1)

Base Information

• Chemical Name: 4(1H)-Pyridinone, 1-hydroxy-3,5-dinitro-, compd. with pyridine (2:1)
• CAS No.: 139055-63-3
• Molecular Formula: C5H5N.2C5H3N3O6
• Molecular Weight: 481.292
• Mol file: 139055-63-3.mol

Synonyms:

Chemical Property of 4(1H)-Pyridinone, 1-hydroxy-3,5-dinitro-, compd. with pyridine (2:1)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4(1H)-Pyridinone, 1-hydroxy-3,5-dinitro-, compd. with pyridine (2:1)

There total 2 articles about 4(1H)-Pyridinone, 1-hydroxy-3,5-dinitro-, compd. with pyridine (2:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

pyridine (110-86-1) + 3,5-dinitro-1-(p-nitrophenyl)-4-pyridone (74197-40-3) → 4-nitro-aniline (100-01-6,104810-17-5) + 1-Hydroxy-3,5-dinitro-1H-pyridin-4-one; compound with pyridine (139055-63-3)

Guidance literature:

With hydroxylamine hydrochloride; at 20 ℃; for 2h;

DOI:10.1246/bcsj.64.3544

Reference yield:

pyridine (110-86-1) + 3,5-dinitro-1-(p-nitrophenyl)-4-pyridone (74197-40-3) → 4-nitro-aniline (100-01-6,104810-17-5) + 4-aci-Nitro-4H-isoxazol-5-one; compound with pyridine + 1-Hydroxy-3,5-dinitro-1H-pyridin-4-one; compound with pyridine (139055-63-3)

Guidance literature:

With hydroxylamine hydrochloride; at 20 ℃; for 2h; Mechanism; Product distribution; other 1-substituted 3,5-dinitro-4-pyridones;

DOI:10.1246/bcsj.64.3544

Reference yield: 80.0%

pyridine (110-86-1) + 1-Hydroxy-3,5-dinitro-1H-pyridin-4-one; compound with pyridine (139055-63-3) → metazonic acid (5653-21-4) + 4-aci-Nitro-4H-isoxazol-5-one; compound with pyridine

Guidance literature:

With hydroxylamine hydrochloride; at 20 ℃; for 2h;

DOI:10.1246/bcsj.64.3544

upstream raw materials:

pyridine

3,5-dinitro-1-(p-nitrophenyl)-4-pyridone

Downstream raw materials:

metazonic acid

Refernces