Trifluoroacetophenone trisylhydrazone

Base Information

• Chemical Name: Trifluoroacetophenone trisylhydrazone
• CAS No.: 127700-40-7
• Molecular Formula: C₂₃H₂₉F₃N₂O₂S
• Molecular Weight: 454.557
• Mol file: 127700-40-7.mol

Synonyms:

Chemical Property of Trifluoroacetophenone trisylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Trifluoroacetophenone trisylhydrazone

There total 1 articles about Trifluoroacetophenone trisylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2,2-Trifluoroacetophenone (434-45-7) + trisylhydrazine (39085-59-1) → Trifluoroacetophenone trisylhydrazone (127700-40-7)

Guidance literature:

With hydrogenchloride; In methanol; Yield given;

DOI:10.1016/S0022-1139(00)81567-5

Reference yield:

Trifluoroacetophenone trisylhydrazone (127700-40-7) → phenyltrifluorodiazoethane (13652-07-8)

Guidance literature:

With potassium hydroxide; In methanol; for 0.0833333h; Heating;

DOI:10.1016/S0022-1139(00)81567-5

Reference yield:

Trifluoroacetophenone trisylhydrazone (127700-40-7) → C26H20F3N2P (127700-50-9)

Guidance literature:

Multi-step reaction with 2 steps

1: KOH / methanol / 0.08 h / Heating

2: diethyl ether

With potassium hydroxide; In methanol; diethyl ether;

DOI:10.1016/S0022-1139(00)81567-5

upstream raw materials:

2,2,2-Trifluoroacetophenone

trisylhydrazine

Downstream raw materials:

phenyltrifluorodiazoethane

C₂₆H₂₀F₃N₂P

Refernces