Technology Process of trans-(S,S)-(+)-4,4'-Bis(3-methylpentyl)azobenzol
There total 8 articles about trans-(S,S)-(+)-4,4'-Bis(3-methylpentyl)azobenzol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
pentane;
at 5 ℃;
for 15h;
Irradiation;
- Guidance literature:
-
Multi-step reaction with 7 steps
2: SOCl2
3: 67 percent / AlCl3
4: 75 percent / 80percent N2H4-H2O, KOH, triethyleneglycol / 1) 2 h, reflux, 2) 4 h, 190 deg C
5: 39 percent / 65percent HNO3 / acetic anhydride / 1) 0 deg C, 2) 50 deg C
6: Zn, NaOH / ethanol; H2O
7: NaOBr / diethyl ether
With
potassium hydroxide; sodium hydroxide; aluminium trichloride; thionyl chloride; sodium hypobromide; nitric acid; hydrazine hydrate; zinc; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol;
In
diethyl ether; ethanol; water; acetic anhydride;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: SOCl2
2: 67 percent / AlCl3
3: 75 percent / 80percent N2H4-H2O, KOH, triethyleneglycol / 1) 2 h, reflux, 2) 4 h, 190 deg C
4: 39 percent / 65percent HNO3 / acetic anhydride / 1) 0 deg C, 2) 50 deg C
5: Zn, NaOH / ethanol; H2O
6: NaOBr / diethyl ether
With
potassium hydroxide; sodium hydroxide; aluminium trichloride; thionyl chloride; sodium hypobromide; nitric acid; hydrazine hydrate; zinc; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol;
In
diethyl ether; ethanol; water; acetic anhydride;
