N^ξ-(2,4-dinitrophenyl)-D-lysine

Base Information

• Chemical Name: N^ξ-(2,4-dinitrophenyl)-D-lysine
• CAS No.: 10466-69-0
• Molecular Formula: C₁₂H₁₆N₄O₆
• Molecular Weight: 312.282
• Mol file: 10466-69-0.mol

Synonyms:

Chemical Property of N^ξ-(2,4-dinitrophenyl)-D-lysine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N^ξ-(2,4-dinitrophenyl)-D-lysine

There total 2 articles about N^ξ-(2,4-dinitrophenyl)-D-lysine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Fmoc-D-Lys(BOC)-OH (92122-45-7) → Nξ-(2,4-dinitrophenyl)-D-lysine (10466-69-0)

Guidance literature:

Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane / 0.5 h

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 20 °C

3: piperidine / N,N-dimethyl-formamide / 0.17 h

With piperidine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/co300110t

Reference yield:

C27H26N4O8 (269061-41-8) → Nξ-(2,4-dinitrophenyl)-D-lysine (10466-69-0)

Guidance literature:

C₂₇H₂₆N₄O₈; With piperidine; In N,N-dimethyl-formamide; for 0.166667h;

With trifluoroacetic acid; In water; acetonitrile;

DOI:10.1021/co300110t

upstream raw materials:

Fmoc-D-Lys(BOC)-OH

C₂₇H₂₆N₄O₈

Refernces