C₂₀H₂₉N₃O₁₁

Base Information

• Chemical Name: C₂₀H₂₉N₃O₁₁
• CAS No.: 1470302-79-4
• Molecular Formula: C₂₀H₂₉N₃O₁₁
• Molecular Weight: 487.464
• Mol file: 1470302-79-4.mol

Synonyms:

Chemical Property of C₂₀H₂₉N₃O₁₁

Chemical Property:

• Boiling Point: 700.6±70.0 °C(Predicted)
• Density: 1.57±0.1 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₀H₂₉N₃O₁₁

There total 6 articles about C₂₀H₂₉N₃O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C27H37N3O14 → C20H29N3O11 (1470302-79-4)

Guidance literature:

With guanidine nitrate; In methanol; dichloromethane;

Reference yield:

3,5-dimethoxy-4-hydroxybenzoic acid (530-57-4) → C20H29N3O11 (1470302-79-4)

Guidance literature:

Multi-step reaction with 5 steps

1: triethylamine; acetic acid / dichloromethane / 5 h

2: diisopropyl-carbodiimide; dmap / dichloromethane / 20 °C

3: tetrabutylammomium bromide; potassium carbonate / chloroform / 45 °C

4: trifluoroacetic acid / dichloromethane

5: guanidine nitrate / dichloromethane; methanol

With dmap; tetrabutylammomium bromide; potassium carbonate; acetic acid; guanidine nitrate; triethylamine; trifluoroacetic acid; diisopropyl-carbodiimide; In methanol; dichloromethane; chloroform;

Reference yield:

N2,N3-bis(tert-butoxycarbonyl)-N1-(4-hydroxybutyl)guanidine (208465-10-5) → C20H29N3O11 (1470302-79-4)

Guidance literature:

Multi-step reaction with 4 steps

1: diisopropyl-carbodiimide; dmap / dichloromethane / 20 °C

2: tetrabutylammomium bromide; potassium carbonate / chloroform / 45 °C

3: trifluoroacetic acid / dichloromethane

4: guanidine nitrate / dichloromethane; methanol

With dmap; tetrabutylammomium bromide; potassium carbonate; guanidine nitrate; trifluoroacetic acid; diisopropyl-carbodiimide; In methanol; dichloromethane; chloroform;

upstream raw materials:

Leonurine

UDP-glucuronic acid

3,5-dimethoxy-4-hydroxybenzoic acid

N²,N³-bis(tert-butoxycarbonyl)-N¹-(4-hydroxybutyl)guanidine

Refernces

• 1、 -. "Leonurine metabolite and preparation method thereof". . . Retrieved 2017/05/02.