2-bromo-1-methoxy-1-phenylpropane

Base Information

• Chemical Name: 2-bromo-1-methoxy-1-phenylpropane
• CAS No.: 102654-45-5
• Molecular Formula: C₁₀H₁₃BrO
• Molecular Weight: 229.117
• Mol file: 102654-45-5.mol

Synonyms:

Chemical Property of 2-bromo-1-methoxy-1-phenylpropane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-bromo-1-methoxy-1-phenylpropane

There total 10 articles about 2-bromo-1-methoxy-1-phenylpropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

methanol (67-56-1) + 1-phenylpropene (637-50-3) → 2-bromo-1-methoxy-1-phenylpropane (102654-45-5)

Guidance literature:

With sodium bromide; at 60 ℃; electrochemical oxidaton: platinum anode, brass cathode;

DOI:10.1007/BF00957466

Reference yield:

→ 2-bromo-1-methoxy-1-phenylpropane (102654-45-5)

Guidance literature:

With chloroform; bromine;

DOI:10.1021/ja01313a071

Reference yield:

1,2-dibromo-1-methoxy-propane (408319-66-4) + phenylmagnesium bromide → 2-bromo-1-methoxy-1-phenylpropane (102654-45-5)

Guidance literature:

With diethyl ether;

upstream raw materials:

methanol

1-phenylpropene

bromotrinitromethane

(1-bromoethyl)benzyl bromide

Downstream raw materials:

(1-methoxyprop-1-en-1-yl)benzene

ephedrine methyl ether

Refernces

• 1、 Niyomura, Osamu,Cox, Matthew,Wirth, Thomas. "Electrochemical generation and catalytic use of selenium electrophiles". . p. 251 - 254. Retrieved 2007/10/03.