4-hydroxy-3,5-di-tert-butylbenzyl alcohol isopropyl ether

Base Information

• Chemical Name: 4-hydroxy-3,5-di-tert-butylbenzyl alcohol isopropyl ether
• CAS No.: 4103-82-6
• Molecular Formula: C₁₈H₃₀O₂
• Molecular Weight: 278.435
• Mol file: 4103-82-6.mol

Synonyms:

Chemical Property of 4-hydroxy-3,5-di-tert-butylbenzyl alcohol isopropyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-hydroxy-3,5-di-tert-butylbenzyl alcohol isopropyl ether

There total 4 articles about 4-hydroxy-3,5-di-tert-butylbenzyl alcohol isopropyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3,5-di-tert-butyl-4-hydroxybenzyl acetate (14387-17-8) + isopropyl alcohol (67-63-0,8013-70-5) → 4-hydroxy-3,5-di-tert-butylbenzyl alcohol isopropyl ether (4103-82-6)

Guidance literature:

With perchloric acid; Heating;

DOI:10.1007/BF00962439

Reference yield:

tris-(3,5-di-tert-butyl-4-hydroxybenzyl)-amine (752-60-3) → 4-hydroxy-3,5-di-tert-butylbenzyl alcohol isopropyl ether (4103-82-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / H₂O / acetone / 1) 1h, reflux, 2) after addition of water 1h, reflux

2: 97 percent / HClO₄ / Heating

With perchloric acid; water; In acetone;

DOI:10.1007/BF00962439

Reference yield:

N,N-dimethyl-(3,5-di-tert-butyl-4-hydroxybenzyl)amine (88-27-7) → 4-hydroxy-3,5-di-tert-butylbenzyl alcohol isopropyl ether (4103-82-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / acetone / Heating

2: 97 percent / HClO₄ / Heating

With perchloric acid; In acetone;

DOI:10.1007/BF00962439

upstream raw materials:

3,5-di-tert-butyl-4-hydroxybenzyl acetate

isopropyl alcohol

tris-(3,5-di-tert-butyl-4-hydroxybenzyl)-amine

N,N-dimethyl-(3,5-di-tert-butyl-4-hydroxybenzyl)amine

Refernces