Technology Process of ethylene glycol bis-(4-fluorosulphonyl-2,3,5,6-tetrafluorobenzoate)
There total 5 articles about ethylene glycol bis-(4-fluorosulphonyl-2,3,5,6-tetrafluorobenzoate) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: aq. NaOH, NaHS / 2 h / 70 °C
2: 978 mg / 30percent H2O2, AcOH / 2 h / 70 °C
3: SOCl2, DMF / 6 h / Heating
4: SF4 / 18 h / 80 °C
5: 1.86 g / 1,1,2-trichloro-1,2,2-trifluoro-ethane / 18 h
With
sodium hydroxide; sodium hydrogensulfide; thionyl chloride; sulfur tetrafluoride; dihydrogen peroxide; acetic acid; N,N-dimethyl-formamide;
In
1,1,2-Trichloro-1,2,2-trifluoroethane;
DOI:10.1016/S0022-1139(00)80200-6
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 978 mg / 30percent H2O2, AcOH / 2 h / 70 °C
2: SOCl2, DMF / 6 h / Heating
3: SF4 / 18 h / 80 °C
4: 1.86 g / 1,1,2-trichloro-1,2,2-trifluoro-ethane / 18 h
With
thionyl chloride; sulfur tetrafluoride; dihydrogen peroxide; acetic acid; N,N-dimethyl-formamide;
In
1,1,2-Trichloro-1,2,2-trifluoroethane;
DOI:10.1016/S0022-1139(00)80200-6
- Guidance literature:
-
Multi-step reaction with 2 steps
1: SF4 / 18 h / 80 °C
2: 1.86 g / 1,1,2-trichloro-1,2,2-trifluoro-ethane / 18 h
With
sulfur tetrafluoride;
In
1,1,2-Trichloro-1,2,2-trifluoroethane;
DOI:10.1016/S0022-1139(00)80200-6
