6-Desoxy-1,3:2,5-di-O-methylen-L-talitol

Base Information

• Chemical Name: 6-Desoxy-1,3:2,5-di-O-methylen-L-talitol
• CAS No.: 55645-89-1
• Molecular Formula: C₈H₁₄O₅
• Molecular Weight: 190.196
• Mol file: 55645-89-1.mol

Synonyms:

Chemical Property of 6-Desoxy-1,3:2,5-di-O-methylen-L-talitol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-Desoxy-1,3:2,5-di-O-methylen-L-talitol

There total 1 articles about 6-Desoxy-1,3:2,5-di-O-methylen-L-talitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 6-Desoxy-1,3:2,5-di-O-methylen-L-talitol (55645-89-1,55660-05-4)

Guidance literature:

2,5:4,6-Di-O-methylen-1-deoxy-L-arabo-3-hexulose, NaBH4, NaOMe, MeOH;

DOI:10.1139/v63-276

Reference yield:

O2,O5;O4,O6-dimethanediyl-1-deoxy-L-mannitol (55645-89-1) → O2,O5-methanediyl-O6-(toluene-4-sulfonyl)-1-deoxy-L-mannitol (898813-90-6)

Guidance literature:

Multi-step reaction with 3 steps

1: acetic acid; sulfuric acid

2: barium methylate; methanol

3: pyridine

With pyridine; methanol; sulfuric acid; barium methoxide; acetic acid;

DOI:10.1021/ja01226a055

Reference yield:

O2,O5;O4,O6-dimethanediyl-1-deoxy-L-mannitol (55645-89-1) → 1-iodo-O2,O5-methanediyl-O3,O4-bis-(toluene-4-sulfonyl)-1,6-dideoxy-L-mannitol (898814-48-7)

Guidance literature:

Multi-step reaction with 4 steps

1: acetic acid; sulfuric acid

2: barium methylate; methanol

3: pyridine

4: sodium iodide; hexane-2,5-dione

With pyridine; methanol; sulfuric acid; barium methoxide; acetic acid; 2,5-hexanedione; sodium iodide;

DOI:10.1021/ja01226a055

Downstream raw materials:

O³-benzoyl-O²,O⁵;O⁴,O⁶-dimethanediyl-1-deoxy-L-mannitol

O²,O⁵;O⁴,O⁶-dimethanediyl-O³-(toluene-4-sulfonyl)-1-deoxy-L-mannitol

O²,O⁵;O⁴,O⁶-dimethanediyl-O³-methyl-1-deoxy-L-mannitol

O³,O⁴,O⁶-triacetyl-O²,O⁵-methanediyl-1-deoxy-L-mannitol