diethyl[N-salicylidene 2-methoxylaniline]gallium

Base Information

• Chemical Name: diethyl[N-salicylidene 2-methoxylaniline]gallium
• CAS No.: 307554-26-3
• Molecular Formula: C₁₈H₂₂GaNO₂
• Molecular Weight: 354.101
• Mol file: 307554-26-3.mol

Synonyms:

Chemical Property of diethyl[N-salicylidene 2-methoxylaniline]gallium

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of diethyl[N-salicylidene 2-methoxylaniline]gallium

There total 1 articles about diethyl[N-salicylidene 2-methoxylaniline]gallium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

N-salicylidene-2-methoxyaniline (3290-98-0,122630-44-8,126183-24-2) + triethyl gallium (1115-99-7) → diethyl[N-salicylidene 2-methoxylaniline]gallium (307554-26-3)

Guidance literature:

In cyclohexane; benzene; byproducts: C2H6; under N2, equimolar amt. of metal-compd. in c-C6H12 was added to 5:1 c-C6H12:C6H6 soln. of Schiff-base over a period of 10 min, stirring for further 5 min at room temp.; solvent was removed in vac., solid was recrystd. from cyclohexane-benzene, elem. anal.;

upstream raw materials:

N-salicylidene-2-methoxyaniline

triethyl gallium

Refernces