triethyl{p-(propylthio)phenyl}germane

Base Information

• Chemical Name: triethyl{p-(propylthio)phenyl}germane
• CAS No.: 131716-92-2
• Molecular Formula: C₁₅H₂₂F₄GeS
• Molecular Weight: 382.989
• Mol file: 131716-92-2.mol

Synonyms:

Chemical Property of triethyl{p-(propylthio)phenyl}germane

Chemical Property:

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Safty Information:

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Technology Process of triethyl{p-(propylthio)phenyl}germane

There total 1 articles about triethyl{p-(propylthio)phenyl}germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

triethylgermylpentafluorobenzene (24692-24-8) + sodium 1-propanethiolate (6898-84-6) → triethyl{p-(propylthio)phenyl}germane (131716-92-2) + 1,2,4,5-tetrafluoro-3-(propylthio)benzene (113827-87-5)

Guidance literature:

In propan-1-ol; 1-propanethiol added to soln. of sodium in PrOH, stirred for 5 min, addn. of germane to the soln. of thiolate, stirred (10h, 20°C); poured into water, extn. with pentane (6h), solvent removed, residue distd. in vac.; elem. anal.;

upstream raw materials:

triethylgermylpentafluorobenzene

sodium 1-propanethiolate