antimony(III) monothiobenzoate

Base Information

• Chemical Name: antimony(III) monothiobenzoate
• CAS No.: 59366-05-1
• Molecular Formula: C₂₁H₁₅O₃S₃Sb
• Molecular Weight: 533.296
• Mol file: 59366-05-1.mol

Synonyms:

Chemical Property of antimony(III) monothiobenzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of antimony(III) monothiobenzoate

There total 2 articles about antimony(III) monothiobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

thiobenzoic acid (98-91-9) + antimony(III) trioxide → antimony(III) monothiobenzoate (59366-05-1)

Guidance literature:

In dichloromethane; stirring (35°C, 3-4 h); evapn., drying (vac.), recrystn. (CH2Cl2); elem. anal.;

DOI:10.1515/znb-1998-1209

Reference yield: 64.0%

thiobenzoic acid (98-91-9) + antimony(III) acetate (6923-52-0) → antimony(III) monothiobenzoate (59366-05-1)

Guidance literature:

In dichloromethane; soln. PhCSOH in CH2Cl2 treated with Sb(CH3COO)3 dissolved in CH2Cl2 andmixt. stirred for 1 h; ppt. filtered, dried and recrystd. from CH2Cl2; elem. anal.;

DOI:10.1016/S0020-1693(00)87680-X

upstream raw materials:

thiobenzoic acid

antimony(III) acetate

thiobenzoic acid

Refernces

• 1、 Singh, Prit,Singh, Sudha,Gupta, Vishnu D.,N?th, Heinrich. "Arsenic(III), Antimony(III) and Bismuth(III) Thiobenzoates: Crystal and Molecular Structures of M(SOCR)3 and PhSb(SOCPh)2". . p. 1475 - 1482. Retrieved 2007/10/03.