Oc₂Sn(N-nitroso-N-phenylhydroxylaminate)2

Base Information

• Chemical Name: Oc₂Sn(N-nitroso-N-phenylhydroxylaminate)2
• CAS No.: 947265-19-2
• Molecular Formula: C₂₈H₄₄N₄O₄Sn
• Molecular Weight: 619.392
• Mol file: 947265-19-2.mol

Synonyms:

Chemical Property of Oc₂Sn(N-nitroso-N-phenylhydroxylaminate)2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Oc₂Sn(N-nitroso-N-phenylhydroxylaminate)2

There total 2 articles about Oc₂Sn(N-nitroso-N-phenylhydroxylaminate)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

cupferron + dioctyltin(IV) oxide (870-08-6) → Oc2Sn(N-nitroso-N-phenylhydroxylaminate)2 (947265-19-2)

Guidance literature:

In methanol; byproducts: NH3; ligand and Sn-complex dissolved in MeOH, stirred and refluxed for 3 h; soln. kept in refrigerator, filtered, solvent slow evapd. at room temp.,washed with MeOH, crystd., recrystd. from hexane or MeOH; elem. anal.;

DOI:10.1016/j.jorganchem.2007.04.003

Reference yield: 64.0%

cupferron + di-n-octyltin dichloride (3542-36-7) → Oc2Sn(N-nitroso-N-phenylhydroxylaminate)2 (947265-19-2)

Guidance literature:

In methanol; byproducts: NH4Cl; ligand and Sn-complex dissolved in MeOH, stirred and refluxed; soln. kept in refrigerator, filtered, crystd., recrystd. from hexane or MeOH; elem. anal.;

DOI:10.1016/j.jorganchem.2007.04.003

upstream raw materials:

dioctyltin(IV) oxide

di-n-octyltin dichloride

Refernces