hexanoic acid-(4-phenylazo-phenacyl ester)

Base Information

• Chemical Name: hexanoic acid-(4-phenylazo-phenacyl ester)
• CAS No.: 102181-73-7
• Molecular Formula: C₂₀H₂₂N₂O₃
• Molecular Weight: 338.406
• Mol file: 102181-73-7.mol

Synonyms:

Chemical Property of hexanoic acid-(4-phenylazo-phenacyl ester)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of hexanoic acid-(4-phenylazo-phenacyl ester)

There total 4 articles about hexanoic acid-(4-phenylazo-phenacyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium caproate (10051-44-2) + 2-bromo-1-(4-phenylazo-phenyl)-ethanone (62625-24-5) → hexanoic acid-(4-phenylazo-phenacyl ester) (102181-73-7)

Guidance literature:

With ethanol;

DOI:10.1021/ac60091a045

Reference yield:

4-acetoazobenzene (4827-16-1) → hexanoic acid-(4-phenylazo-phenacyl ester) (102181-73-7)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid; bromine / 75 °C

2: aqueous ethanol

With ethanol; bromine; acetic acid;

Reference yield:

4-phenylazobenzoyl chloride (104-24-5) → hexanoic acid-(4-phenylazo-phenacyl ester) (102181-73-7)

Guidance literature:

Multi-step reaction with 3 steps

1: diethyl ether

2: HBr; CHCl₃

3: aqueous ethanol

With diethyl ether; ethanol; chloroform; hydrogen bromide;

upstream raw materials:

sodium caproate

2-bromo-1-(4-phenylazo-phenyl)-ethanone

4-acetoazobenzene

4-phenylazobenzoyl chloride