Technology Process of C24H26BrClF3N7O3
There total 3 articles about C24H26BrClF3N7O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tert.-butylhydroperoxide; water-d2; toluene-4-sulfonic acid; zinc(II) chloride;
In
chloroform;
at 50 ℃;
for 8h;
Cooling with ice;
DOI:10.1021/ja407739y
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydride; ethanethiol / tetrahydrofuran / 12 h / 0 °C / Inert atmosphere
2: toluene-4-sulfonic acid; zinc(II) chloride; tert.-butylhydroperoxide; water-d2 / chloroform / 8 h / 50 °C / Cooling with ice
With
tert.-butylhydroperoxide; water-d2; sodium hydride; toluene-4-sulfonic acid; ethanethiol; zinc(II) chloride;
In
tetrahydrofuran; chloroform;
DOI:10.1021/ja407739y
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium azide; sodium iodide / N,N-dimethyl-formamide / 10 h / 65 °C / Inert atmosphere
2: sodium hydride; ethanethiol / tetrahydrofuran / 12 h / 0 °C / Inert atmosphere
3: toluene-4-sulfonic acid; zinc(II) chloride; tert.-butylhydroperoxide; water-d2 / chloroform / 8 h / 50 °C / Cooling with ice
With
tert.-butylhydroperoxide; sodium azide; water-d2; sodium hydride; toluene-4-sulfonic acid; ethanethiol; sodium iodide; zinc(II) chloride;
In
tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/ja407739y