C₃₅H₃₂N₂

Base Information

• Chemical Name: C₃₅H₃₂N₂
• CAS No.: 1346231-30-8
• Molecular Formula: C₃₅H₃₂N₂
• Molecular Weight: 480.652
• Mol file: 1346231-30-8.mol

Synonyms:

Chemical Property of C₃₅H₃₂N₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₅H₃₂N₂

There total 5 articles about C₃₅H₃₂N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-diphenylaminobenzene (603-34-9) → C35H32N2 (1346231-30-8)

Guidance literature:

Multi-step reaction with 4 steps

1.1: trichlorophosphate / 1 h / 0 °C / Inert atmosphere

1.2: 4 h / 105 °C / Inert atmosphere

2.1: sodium tetrahydroborate / ethanol / 3 h / 0 - 20 °C

3.1: N-ethyl-N,N-diisopropylamine / 2 h / 0 - 40 °C

4.1: Diphenyliodonium 9,10-dimethoxyanthracene-2-sulfonate / UV-irradiation

With sodium tetrahydroborate; Diphenyliodonium 9,10-dimethoxyanthracene-2-sulfonate; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In ethanol; 1.1: Vilsmeier formylation / 1.2: Vilsmeier formylation / 4.1: Friedel Crafts alkylation;

DOI:10.1021/ma2018217

Reference yield:

4,4'-diformyltriphenylamine (53566-95-3) → C35H32N2 (1346231-30-8)

Guidance literature:

Multi-step reaction with 4 steps

1: trichlorophosphate / 1 h / 105 °C / Cooling with ice

2: sodium tetrahydroborate / ethanol / 3 h / 0 - 20 °C

3: N-ethyl-N,N-diisopropylamine / 2 h / 0 - 40 °C

4: Diphenyliodonium 9,10-dimethoxyanthracene-2-sulfonate / UV-irradiation

With sodium tetrahydroborate; Diphenyliodonium 9,10-dimethoxyanthracene-2-sulfonate; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In ethanol; 1: Vilsmeier formylation / 4: Friedel Crafts alkylation;

DOI:10.1021/ma2018217

Reference yield:

tris(4-formylphenyl)amine (119001-43-3) → C35H32N2 (1346231-30-8)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium tetrahydroborate / ethanol / 3 h / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine / 2 h / 0 - 40 °C

3: Diphenyliodonium 9,10-dimethoxyanthracene-2-sulfonate / UV-irradiation

With sodium tetrahydroborate; Diphenyliodonium 9,10-dimethoxyanthracene-2-sulfonate; N-ethyl-N,N-diisopropylamine; In ethanol; 3: Friedel Crafts alkylation;

DOI:10.1021/ma2018217

upstream raw materials:

9-butyl-9H-carbazole

4,4',4''-tris(acetoxymethylene)triphenylamine

N,N-diphenylaminobenzene

4,4'-diformyltriphenylamine

Refernces