Sn(n-Bu)2Cl₂*H₂-3-MeOsalen

Base Information

• Chemical Name: Sn(n-Bu)2Cl₂*H₂-3-MeOsalen
• CAS No.: 674798-79-9
• Molecular Formula: C₂₆H₃₈Cl₂N₂O₄Sn
• Molecular Weight: 632.215
• Mol file: 674798-79-9.mol

Synonyms:

Chemical Property of Sn(n-Bu)2Cl₂*H₂-3-MeOsalen

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of Sn(n-Bu)2Cl₂*H₂-3-MeOsalen

There total 1 articles about Sn(n-Bu)2Cl₂*H₂-3-MeOsalen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

N,N'-bis(3-methoxysalicylidene)ethylenediamine (7396-77-2) + dibutyltin chloride (683-18-1) → Sn(n-Bu)2Cl2*H2-3-MeOsalen (674798-79-9)

Guidance literature:

In acetonitrile; 1 equiv. of H2-3-MeOsalen was added to a MeCN soln. of Bu2SnCl2, the mixt. was stirred over gentle heat for 1 h; cooled, ppt. of the adduct was filtd. off, mother liquor was left standing for ca. 12 h to give the crystals of X-ray quality; elem. anal.;

DOI:10.1021/om030540f

upstream raw materials:

N,N'-bis(3-methoxysalicylidene)ethylenediamine

dibutyltin chloride

Refernces