Technology Process of KCo(m-chlorophenolate)3(tetrahydrofuran)*(tetrahydrofuran)
There total 2 articles about KCo(m-chlorophenolate)3(tetrahydrofuran)*(tetrahydrofuran) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
tetrahydrofuran;
byproducts: KBr; under abs. water free conditions (anaerobic conditions) in Ar atm. usingSchlenk techniques; mixt. of ligand and Co salt (molar ratio >=4) stirr ed at room temp. for 0.5-2 h; allowed to stand for 24 h; KBr filtered under Ar atm.; filtrate concd. (vac.) at room temp. or at temp. max. 40°C; concd. soln. was left for 10 ds at -78°C; n-hexane added; complex filtered under Ar atm.; washed (dry THF); dried (vac.); elem. anal.;
DOI:10.1016/j.saa.2006.11.015
- Guidance literature:
-
In
neat (no solvent);
under abs. water free conditions (anaerobic conditions) in Ar atm. usingSchlenk techniques; under the presence of THF vapour for several hs or ds; elem. anal.;
DOI:10.1016/j.saa.2006.11.015
