C₁₇H₁₇N₃O₂S₃

Base Information

• Chemical Name: C₁₇H₁₇N₃O₂S₃
• CAS No.: 1369585-73-8
• Molecular Formula: C₁₇H₁₇N₃O₂S₃
• Molecular Weight: 391.539
• Mol file: 1369585-73-8.mol

Synonyms:

Chemical Property of C₁₇H₁₇N₃O₂S₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₁₇N₃O₂S₃

There total 2 articles about C₁₇H₁₇N₃O₂S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-ethyl-N-phenylthiourea (3955-58-6) + phenyl isothiocyanate (103-72-0) + methanesulfonyl chloride (124-63-0) → C17H17N3O2S3 (1369585-73-8)

Guidance literature:

N-ethyl-N-phenylthiourea; phenyl isothiocyanate; With sodium hydride; In tetrahydrofuran; paraffin oil; at 45 ℃; Inert atmosphere;

With hydrogen bromide; dihydrogen peroxide; In tetrahydrofuran; paraffin oil; Inert atmosphere;

methanesulfonyl chloride; Further stages;

DOI:10.1055/s-0031-1290124

Reference yield:

N-ethyl-N-phenylamine (103-69-5) → C17H17N3O2S3 (1369585-73-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: hydrogenchloride / water / Reflux

2.1: sodium hydride / tetrahydrofuran; paraffin oil / 45 °C / Inert atmosphere

2.2: Inert atmosphere

With hydrogenchloride; sodium hydride; In tetrahydrofuran; water; paraffin oil;

DOI:10.1055/s-0031-1290124

upstream raw materials:

N-ethyl-N-phenylthiourea

phenyl isothiocyanate

methanesulfonyl chloride

N-ethyl-N-phenylamine

Refernces