C₂₃H₂₆N₈OS

Base Information

• Chemical Name: C₂₃H₂₆N₈OS
• CAS No.: 1607479-53-7
• Molecular Formula: C₂₃H₂₆N₈OS
• Molecular Weight: 462.578
• Mol file: 1607479-53-7.mol

Synonyms:

Chemical Property of C₂₃H₂₆N₈OS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₂₆N₈OS

There total 3 articles about C₂₃H₂₆N₈OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-dichloro-6-methylthieno[2,3-d]pyrimidine (76872-23-6) → C23H26N8OS (1607479-53-7)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonium hydroxide / tetrahydrofuran / 25 °C

2: N,N-dimethyl-formamide / 100 - 180 °C / Microwave irradiation; Alkaline conditions

With ammonium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2014.03.052

Reference yield:

2-amino-5-methylthiophene-3-carbonitrile (138564-58-6) → C23H26N8OS (1607479-53-7)

Guidance literature:

Multi-step reaction with 3 steps

1: acetonitrile / 15 h / 100 °C / Sealed tube

2: ammonium hydroxide / tetrahydrofuran / 25 °C

3: N,N-dimethyl-formamide / 100 - 180 °C / Microwave irradiation; Alkaline conditions

With ammonium hydroxide; acetonitrile; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2014.03.052

Reference yield:

1-(7(R)-methyl-1,4-diazepan-1-yl)-1-[5-methyl-2-(2H-1,2,3-triazole-2-yl)phenyl]methanone (1030377-32-2) + C7H6ClN3S (87478-90-8) → C23H26N8OS (1607479-53-7)

Guidance literature:

In N,N-dimethyl-formamide; at 100 - 180 ℃; Microwave irradiation; Alkaline conditions;

DOI:10.1016/j.bmcl.2014.03.052

upstream raw materials:

2,4-dichloro-6-methylthieno[2,3-d]pyrimidine

1-(7(R)-methyl-1,4-diazepan-1-yl)-1-[5-methyl-2-(2H-1,2,3-triazole-2-yl)phenyl]methanone

C₇H₆ClN₃S

2-amino-5-methylthiophene-3-carbonitrile

Refernces