4-nitro-benzenesulfonic acid octadecylamide

Base Information

• Chemical Name: 4-nitro-benzenesulfonic acid octadecylamide
• CAS No.: 103168-51-0
• Molecular Formula: C₂₄H₄₂N₂O₄S
• Molecular Weight: 454.674
• Mol file: 103168-51-0.mol

Synonyms:

Chemical Property of 4-nitro-benzenesulfonic acid octadecylamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-nitro-benzenesulfonic acid octadecylamide

There total 2 articles about 4-nitro-benzenesulfonic acid octadecylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-aminooctadecane (124-30-1) + 4-Nitrobenzenesulfonyl chloride (98-74-8) → 4-nitro-benzenesulfonic acid octadecylamide (103168-51-0)

Guidance literature:

With triethylamine; In dichloromethane; for 4h; Cooling with ice;

DOI:10.1002/cbic.202100672

Reference yield:

→ 4-nitro-benzenesulfonic acid octadecylamide (103168-51-0)

Guidance literature:

/BRN= 3466968/;

Reference yield:

4-nitro-benzenesulfonic acid octadecylamide (103168-51-0) → N-hexadecyloctadecan-1-amine (45310-14-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C

2: potassium carbonate; 2-hydroxyethanethiol / N,N-dimethyl-formamide / 6 h / 20 °C

With potassium carbonate; 2-hydroxyethanethiol; In N,N-dimethyl-formamide;

DOI:10.1002/cbic.202100672

upstream raw materials:

1-aminooctadecane

4-Nitrobenzenesulfonyl chloride

Downstream raw materials:

N-hexadecyloctadecan-1-amine

Refernces