C₂₉H₂₅BrN₄

Base Information

• Chemical Name: C₂₉H₂₅BrN₄
• CAS No.: 1313190-73-6
• Molecular Formula: C₂₉H₂₅BrN₄
• Molecular Weight: 509.448
• Mol file: 1313190-73-6.mol

Synonyms:

Chemical Property of C₂₉H₂₅BrN₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₂₅BrN₄

There total 1 articles about C₂₉H₂₅BrN₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

α-Benzoyl-(4-brombenzyliden)-aceton (72200-92-1,72758-34-0) + phenylhydrazine (100-63-0) → C29H25BrN4 (1313190-73-6)

Guidance literature:

With hydrogenchloride; In ethanol; water; Reflux;

DOI:10.1080/15533174.2011.591645

Reference yield: 81.0%

lanthanum(III) nitrate hexahydrate + C29H25BrN4 (1313190-73-6) → [lanthanum(III)(BrC6H4CHC(C(Me)NNHPh)(C(Ph)NNHPh)(nitrate)(H2O)3](nitrate)2

Guidance literature:

With Theil buffer; In ethanol; soln. of BrC6H4CHC(C(Me)NNHPh)(C)PH)NNHPh) (5 mmol) and La(NO3)3*6H2O (7mmol) refluxed for 12 h at pH=6.5-7.8 (adjusted with Theil buffer), coo led to room temp.; filtered, washed with EtOH and H2O, recrystd. from EtOH, dried in desiccator; elem. anal.;

DOI:10.1080/15533174.2011.591645

Reference yield: 54.0%

scandium(III) nitrate hydrate + C29H25BrN4 (1313190-73-6) → [scandium(III)(BrC6H4CHC(C(Me)NNHPh)(C(Ph)NNHPh)(nitrate)(H2O)3](nitrate)2

Guidance literature:

With Theil buffer; In ethanol; soln. of BrC6H4CHC(C(Me)NNHPh)(C)PH)NNHPh) (5 mmol) and Sc(NO3)3*(x)H2O (7 mmol) refluxed for 12 h at pH=6.5-7.8 (adjusted with Theil buffer), cooled to room temp.; filtered, washed with EtOH and H2O, recrystd. from EtOH, dried in desiccator; elem. anal.;

DOI:10.1080/15533174.2011.591645

upstream raw materials:

α-Benzoyl-(4-brombenzyliden)-aceton

phenylhydrazine

Refernces