Technology Process of 2,2′,2″,2?-(porphine-5,10,15,20-tetrayl)tetrakis(methyl benzoate)
There total 7 articles about 2,2′,2″,2?-(porphine-5,10,15,20-tetrayl)tetrakis(methyl benzoate) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
pyrrole; methyl o-formylbenzoate;
With
boron trifluoride diethyl etherate;
In
dichloromethane;
at 20 ℃;
for 2h;
Schlenk technique;
Inert atmosphere;
Darkness;
With
2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane;
at 20 ℃;
for 1h;
Schlenk technique;
Inert atmosphere;
DOI:10.1039/c8cy02164c
- Guidance literature:
-
With
2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; water;
for 0.5h;
Yield given;
DOI:10.1021/jo9600161
- Guidance literature:
-
Multi-step reaction with 2 steps
1: aq. sodium dodecyl sulfate, HCl / 2 h
2: 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / H2O; tetrahydrofuran / 0.5 h
With
hydrogenchloride; sodium dodecyl-sulfate; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; water;
DOI:10.1021/jo9600161
