<2>Thienyl-phenyl-zink

Base Information

• Chemical Name: <2>Thienyl-phenyl-zink
• CAS No.: 46116-42-1
• Molecular Formula: C₁₀H₈SZn
• Molecular Weight: 225.63
• Mol file: 46116-42-1.mol

Synonyms:

Chemical Property of <2>Thienyl-phenyl-zink

Chemical Property:

Purity/Quality:

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Technology Process of <2>Thienyl-phenyl-zink

There total 1 articles about <2>Thienyl-phenyl-zink which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ <2>Thienyl-phenyl-zink (46116-42-1)

Guidance literature:

Phenylzinkjodid-aetherat, <2>Thienylmagnesiumjodid;

Reference yield: 83.0%

<2>Thienyl-phenyl-zink (46116-42-1) + 1-(2,4-dinitrophenoxy)piperidine (110210-11-2) → 1-(thiophen-2-yl)piperidine (19983-20-1)

Guidance literature:

With nickel(II) chloride hexahydrate; 4,4'-di-tert-butyl-2,2'-bipyridine; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 1h; Sealed tube; Inert atmosphere;

DOI:10.1002/anie.201900510

Downstream raw materials:

1-(thiophen-2-yl)piperidine