13,13'-bis(dibenzofluorenyl)

Base Information

• Chemical Name: 13,13'-bis(dibenzofluorenyl)
• CAS No.: 120908-27-2
• Molecular Formula: C₄₂H₂₆
• Molecular Weight: 530.668
• Mol file: 120908-27-2.mol

Synonyms:

Chemical Property of 13,13'-bis(dibenzofluorenyl)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 13,13'-bis(dibenzofluorenyl)

There total 2 articles about 13,13'-bis(dibenzofluorenyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

bis(1-naphthyl)methanol (62784-66-1) → 1,1'-dinaphthylmethane (607-50-1) + 13H-dibenzo[a,i]fluorene (239-60-1) + 13,13'-bis(dibenzofluorenyl) (120908-27-2) + 13H-13-dibenzofluorene (216393-39-4)

Guidance literature:

With phosphoric acid; for 1h; Heating; other reagent: trifluoromethanesulfonic acid;

DOI:10.1021/jo981397g

Reference yield: 8.0%

13H-13-dibenzofluorene (216393-39-4) → 1,1'-dinaphthylmethane (607-50-1) + 13H-dibenzo[a,i]fluorene (239-60-1) + 1,1,2,2-tetra(1-naphthyl)ethane (152635-71-7) + 13,13'-bis(dibenzofluorenyl) (120908-27-2)

Guidance literature:

With phosphoric acid; at 240 ℃; for 2.5h; Product distribution; Mechanism; other reagent: AlCl₃, reagent absence, solvents: naphthalene, benzene, CS₂, other temperature and time;

DOI:10.1021/jo981397g

upstream raw materials:

bis(1-naphthyl)methanol

13H-13-dibenzofluorene

Refernces