Technology Process of 2-(hydroxymethyl)-1,4-naphthoquinone N-methylcarbamate
There total 5 articles about 2-(hydroxymethyl)-1,4-naphthoquinone N-methylcarbamate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 49 percent / N-bromosuccinimide, azobis(2-methylpropionitrile), Ac2O / 0.5 h / 120 - 130 °C
2: 50 percent / CHCl3; acetic acid / 95 - 100 °C
3: 20 percent / CF3COOH, H2O / 1.5 h / Heating
4: 36 percent / CH2Cl2 / 24 h / Heating
With
N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); water; acetic anhydride; trifluoroacetic acid;
In
dichloromethane; chloroform; acetic acid;
DOI:10.1021/jm00348a023
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 50 percent / CHCl3; acetic acid / 95 - 100 °C
2: 20 percent / CF3COOH, H2O / 1.5 h / Heating
3: 36 percent / CH2Cl2 / 24 h / Heating
With
water; trifluoroacetic acid;
In
dichloromethane; chloroform; acetic acid;
DOI:10.1021/jm00348a023
